Self-Propagating High Temperature Synthesis of Composite Material Based on Zirconium and Chromum Oxide

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Resumo

Ceramic composite materials based on stabilized zirconium oxide were obtained by self-propagating high-temperature synthesis. Yttrium oxide was used as a stabilizing additive. The work studied the effect of the content of yttrium oxide additive on the temperature and combustion rate of the materials studied. Also, based on the results of X-ray phase analysis and scanning electron microscopy, the effect of yttrium oxide on the phase composition and microstructure of the synthesized materials was studied.

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Sobre autores

A. Chizhikov

Merzhanov Institute of Structural Macrokinetics and Materials Science of the Russian Academy of Sciences (ISMAN)

Autor responsável pela correspondência
Email: chij@ism.ac.ru
ORCID ID: 0000-0003-2793-6952
Rússia, Chernogolovka, 142432

М. Антипов

Merzhanov Institute of Structural Macrokinetics and Materials Science of the Russian Academy of Sciences (ISMAN)

Email: chij@ism.ac.ru
ORCID ID: 0000-0002-7498-428X
Rússia, Chernogolovka, 142432

A. Konstantinov

Merzhanov Institute of Structural Macrokinetics and Materials Science of the Russian Academy of Sciences (ISMAN)

Email: chij@ism.ac.ru
ORCID ID: 0000-0002-0524-6283
Rússia, Chernogolovka, 142432

A. Zhidovich

Merzhanov Institute of Structural Macrokinetics and Materials Science of the Russian Academy of Sciences (ISMAN)

Email: chij@ism.ac.ru
Rússia, Chernogolovka, 142432

P. Bazhin

Merzhanov Institute of Structural Macrokinetics and Materials Science of the Russian Academy of Sciences (ISMAN)

Email: chij@ism.ac.ru
ORCID ID: 0000-0003-1710-3965
Rússia, Chernogolovka, 142432

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2. Fig. 1. Diagram of the state of the ZrO2–Y2O3 system [35] (a) and the dependence of the temperature (1) and gorenje rate of the studied materials (2) on the content of Y2O3 (b).

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3. Fig. 2. The scheme of experiments to measure the combustion characteristics of the studied materials: 1 – the initial blank, 2 – asbestos insulation, 3 – quartz glass, 4 - ceramic tube, 5 – thermocouples, 6 – initiating spiral, 7 – substrate. Gorenje.

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4. Fig. 3. X-ray images of samples No. 0, 1, 5, 9.

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5. Fig. 4. SEM results of the obtained composite materials: (a), (c) – morphology of powders of compositions 0 and 5; (b), (d) – microstructure of powders of compositions 0 and 5; (e) – microstructure and results of EDA analysis of sample 9. Results EDAS are given in % by weight.

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