SYNTHESIS AND STUDY OF SUBMICRON BARIUM HEXAFERRITE CERAMICS OBTAINED BY LIQUID-PHASELOW-TEMPERATURE SINTERING OF BaFe12O19 NANOPARTICLES

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Abstract

In this work, the problem of obtaining ceramic samples of barium hexaferrite BaFe12O19 with high values of coercivity was being solved. For this purpose, BaFe12O19 nanopowder with coercivity Hc=445 kA/m was synthesized by hydrothermal synthesis. Sintering was carried out at low temperature (900∘C) to preserve the grains in a single-domain state. To perform sintering at such a low temperature, B2O3 or Bi2O3 was added to the hexaferrite. The effect of the amount and type of additive on the phase composition, microstructure and magnetic properties of sintered hexaferrite was studied. It was shown that using Bi2O3(in the form of 0.5, 1 or 3 wt.% of Bi(NO3)3) led to no changes in the phase composition, while addition of B2O3(in the form of 0.5, 1 or 3 wt.% of H3BO3) resulted in partial transformation of hexaferrite into hematite α-Fe2O3. It was found that with increasing concentration of Bi2O3 or B2O3, the average grain size of BaFe12O19 increases,but does not exceed the critical single-domain size. This provides high Hcvalues of the sintered samples (370-420 kA/m), which makes them superior to most well-known brands of unsubstituted hexaferrites.

About the authors

A. Yu. Mironovich

National University of Science & Technology “MISIS”

Email: amironovich24@gmail.ru
Moscow, Russia

V. G. Kostishyn

National University of Science & Technology “MISIS”

Moscow, Russia

H. I. Al-Khafaji

National University of Science & Technology “MISIS”

Moscow, Russia

A. V. Timofeev

National University of Science & Technology “MISIS”

Moscow, Russia

E. S. Savchenko

National University of Science & Technology “MISIS”

Moscow, Russia

A. I. Ril

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Moscow, Russia

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