Extraction of Pb2+ Ions By Sodium Aluminosilicates Synthesized From Rice Straw

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Abstract

Samples of sodium aluminosilicates obtained by hydrolytic deposition using rice straw of different varieties as silicon-containing raw materials were studied. The morphology of the particles was determined by scanning electron microscopy, the specific surface area (362–470 m2/g) was measured, IR spectra were recorded, and the chemical and phase composition of the samples was determined. The sorption properties of the obtained materials with respect to lead ions have been studied, the sorption capacity is 199–550 mg/g. An organic component was found and isolated in the samples, which is formed as a result of the deposition of aluminosilicates from rice straw hydrolysates, its composition was determined by thermogravimetry and IR spectroscopy. The effect of the organic component on the sorption capacity of plant-derived aluminosilicates has been investigated. The proposed sorption mechanism has been established. The approach used makes it possible to obtain aluminosilicates with a high sorption capacity, as well as safely dispose of rice straw.

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About the authors

A. N. Kholomeydik

Institute of Chemistry, Far-Eastern Branch, Russian Academy of Sciences

Author for correspondence.
Email: anik@ich.dvo.ru
Russian Federation, Vladivostok, 690022

A. E. Panasenko

Institute of Chemistry, Far-Eastern Branch, Russian Academy of Sciences

Email: anik@ich.dvo.ru
Russian Federation, Vladivostok, 690022

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Supplementary files

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2. Fig. 1. IR spectra: 1 — sample 1 (numbering according to Table. 1); 2 — KAlSi3O8 · nH2O aluminosilicate.

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3. Fig. 2. Typical radiograph of samples 1-3 (numbering according to Table 1).

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4. Fig. 3. Micrographs of samples 1-3 (numbering according to Table 1).

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5. Fig. 4. Thermogram of sample 1 (numbering according to Table 1).

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6. Fig. 5. Isotherms of lead adsorption in samples 1-3 (numbering according to Table 1).

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7. Fig. 6. The IR spectrum of the isolated organic component of the studied samples of aluminosilicate materials.

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